QUOTE(deepdiver32073)Go to
www.sciencelab.com
they have just about everything a budding "chemist" might want or need. That's where I got my last batch. Can I ask what you want/need it for? That's pretty nasty stuff that'll eat you up if you're not careful. There are also different grades of purity, so if what you're making requires absolute purity (nitroglycerine for example) you'll pay for the extra purity. Otherwise, it's not too expensive.
Actually had a look at these guys before, except sadly they don't ship out of the US..
And "Nitric Acid, Reagent, ACS: 25 ml 1 $17.00 " is fine for what I'm doing..
QUOTE(raum)whoami, if you are worried about the cost of nitric acid, that means you don't got the scratch to afford the protective equipment and safety gear. leave this alone if you can't do it right.
and you want baking soda around at all times you are working with nitric acid.
OK, technically, I'm not actually worried at the cost of the acid itself, more where I can obtain it in Australia without having to ordering $5000 minimum quantity..
Also, I'm not really one to cut back on the safety equipment - plus, for what I'm making, I'm gonna have to stay the fuck back.. lol
Also, to tell you the truth, I'd rather just purchase the chemical in it's purified form rather than read a synthesis..
So, if I were living in the states, I would buy it from ScienceLab at $40 for 500g - more that I need, lol
QUOTE(deepdiver32073)And water.
As far as protective equipment, at a MINIMUM you need acid proof gloves, acid proof apron, and acid proof eye protection. DO NOT USE LATEX GLOVES! They will melt onto and into your skin. I strongly recommend Pyrex glassware or something similar. A workbench that is at a comfortable height with access to running water is also very important.
See above - I wasn't planning on cutting back on the protective equipment, or quality lab equipment.
(and lets hope when you said water, you meant only when and if I get the acid on myself, lol)
QUOTE(deepdiver32073)Man, I remember once in HS this chick spilled a beaker of aqua regia (hot nitric & sulfuric acid mixed) in her lap then raised hell when the instructor grabbed her, tossed her under the safety shower and yanked her pantyhose off. She quieted down when the burns on her legs appeared and she saw the melted hose. Her dad later tried to sue the school and the teacher for "humiliating" his little girl, but dropped it when all 30 of us in the lab signed up to testify.
LMAO..!!
Well, I think that that sorta reponds to the 6 replies - except Pete's which I'd like to keep from you for a small while, hehe..
I might actually end up just using some low-grade sulfuric acid, and make a completely different compound.. (but I expect it'll affect the yield somewhat)
Even looking in the Yellow Pages for a chemical supplier is just too damn hard..
Oh, and if you're still wondering - here's a clue:
(not that I expect that helps - doesn't help me, lol)